Introduction to Organic Laboratory Techniques : A Microscale Approach by George
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Introduction to Organic Laboratory Techniques : A Microscale Approach by George
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eBay-Artikelnr.:176632964904
Artikelmerkmale
- Artikelzustand
- ISBN
- 9780495016304
Über dieses Produkt
Product Identifiers
Publisher
Brooks/Cole
ISBN-10
0495016306
ISBN-13
9780495016304
eBay Product ID (ePID)
48321581
Product Key Features
Number of Pages
1008 Pages
Language
English
Publication Name
Introduction to Organic Laboratory Techniques : a Microscale Approach
Publication Year
2006
Subject
General, Chemistry / Organic, Chemistry / Inorganic
Type
Textbook
Subject Area
Education, Science
Format
Hardcover
Dimensions
Item Height
1.3 in
Item Weight
71.4 Oz
Item Length
11 in
Item Width
8.7 in
Additional Product Features
Edition Number
4
Intended Audience
College Audience
LCCN
2005-938320
Illustrated
Yes
Table Of Content
Part One: INTRODUCTION TO BASIC LABORATORY TECHNIQUES.Experiment 1: Introduction to Microscale Laboratory.Experiment 2: Solubility.Experiment 3: Crystallization.Experiment 4: Extraction.Experiment 5: Chromatography.Experiment 6: Simple and Fractional Distillation.Experiment 6A: Simple and Fractional Distillation (Semi-Microscale Procedure).Experiment 6B: Simple and Fractional Distillation (Microscale Procedure).Experiment 7: Infrared Spectroscopy and Boiling-Point Elevation.Essay Aspirin.Experiment 8: Acetylsalicylic Acid.Essay Analgesics.Experiment 9: Isolation of the Active Ingredient in an Analgesic Drug.Experiment 10: Acetaminophen.Experiment 10A: Acetaminophen (Microscale Procedure).Experiment 10B: Acetaminophen (Semi-Microscale Procedure).Essay Identification of Drugs.Experiment 11: TLC Analysis of Analgesic Drugs.Essay Caffeine.Experiment 12: Isolation of Caffeine from Tea or Coffee.Experiment 12A: Extraction of Caffeine from Tea with Methylene Chloride.Experiment 12B: Extraction of Caffeine from Tea or Coffee Using Solid Phase Extraction (SPE).Essay Esters¡XFlavors and Fragrances.Experiment 13: Isopentyl Acetate (Banana Oil).Experiment 13A: Isopentyl Acetate (Microscale Procedure).Experiment 12B: Isopentyl Acetate (Semi-Microscale Procedure).Essay Terpenes and Phenylpropanoids.Experiment 14: Essential Oils: Extractions of Oil from Cloves by Steam Distillation and Liquid Carbon Dioxide.Experiment 14A: Oil of Cloves (Microscale Procedure).Experiment 14B: Oil of Cloves (Semi-Microscale Procedure).Experiment 14C: Extraction of Oil of Cloves with Liquid Carbon Dioxide.Essay Stereochemical Theory of Odor.Experiment 15: Spearmint and Caraway Oil: ()- and ()-Carvones.Essay The Chemistry of Vision.Experiment 16: Isolation of Chlorophyll and Carotenoid Pigments from Spinach.Essay Ethanol and Fermentation Chemistry.Experiment 17: Ethanol from Sucrose.Part Two: INTRODUCTION TO MOLECULAR MODELING.Essay Molecular Modeling and Molecular Mechanics.Experiment 18: An Introduction to Molecular Modeling.Experiment 18A: The Conformations of n-Butane: Local Minima.Experiment 18B: Cyclohexane Chair and Boat Conformations.Experiment 18C: Substituted Cyclohexane Rings.Experiment 18D: cis- and trans-2-Butene.Essay Computational Chemistry¡Vab Initio and Semiempirical Methods.Experiment 19: Computational Chemistry.Experiment 19A: Heats of Formation: Isomerism, Tautomerism, and Regioselectivity.Experiment 19B: Heats of Reaction: SN1 Reaction Rates.Experiment 19C: Density¡VElectrostatic Potential Maps¡XAcidities of Carboxylic Acids.Experiment 19D: Density¡VElectrostatic Potential Maps: Carbocations.Experiment 19E: Density¡VLUMO Maps: Reactivities of Carbonyl Groups.Part Three: PREPARATIONS AND REACTIONS OF ORGANIC COMPOUNDS.Experiment 20: Reactivities of Some Alkyl Halides.Experiment 21: Nucleophilic Substitution Reactions: Competing Nucleophiles.Experiment 21A: Competitive Nucleophiles with 1-Butanol or 2-Butanol.Experiment 21B: Competitive Nucleophiles with 2-Methyl-2-propanol.Experiment 21C: Analysis.Experiment 22: Hydrolysis of Some Alkyl Chlorides.Experiment 23: Synthesis of n-Butyl Bromide and t-Pentyl Chloride.Experiment 23A: n-Butyl Bromide.Experiment 23B: n-Butyl Bromide (Semi-Microscale Procedure).Experiment 23C: t-Pentyl Chloride (Microscale Procedure).Experiment 23D: t-Pentyl Chloride (Semi-Microscale Procedure).Experiment 23E: t-Pentyl Chloride (Macroscale Procedure).Experiment 24: Elimination Reactions: Dehydration and Dehydrohalogenation.Experiment 24A: Dehydration of 1-Butanol and 2-Butanol.Experiment 24B: Dehydrobromination of 1-Bromobutane and 2-Bromobutane.Experiment 25: 4-Methylcyclohexene.Experiment 25A: 4-Methylcyclohexene (Microscale Procedure).Experiment 25B: 4-Methylcyclohexene (Semi-Microscale Procedure).Experiment 26: Phase-Transfer Catalysis: Addition of Dichlorocarbene to Cyclohexene.Experiment 27: Relative Reactivities of Several Aromatic Compounds
Synopsis
In this laboratory textbook for students of organic chemistry, experiments are designed to utilize microscale glassware and equipment. The textbook features a large number of traditional organic reactions and syntheses, as well as the isolation of natural products and experiments with a biological or health sciences focus. The organization of the text is based on essays and topics of current interest. The lab manual contains a comprehensive treatment of laboratory techniques.
LC Classification Number
QD261.I54 2007
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