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NMR - Von Spektren zu Strukturen: Ein experimenteller Ansatz von Terence N. Mitchel

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ISBN-13
9783540721956
Book Title
NMR - From Spectra to Structures
ISBN
9783540721956
Publication Name
NMR-From Spectra to Structures : an Experimental Approach
Item Length
9.3in
Publisher
Springer Berlin / Heidelberg
Publication Year
2007
Type
Textbook
Format
Trade Paperback
Language
English
Item Height
0.2in
Author
Burkhard Costisella, Terence N. Mitchell
Features
Revised
Item Width
6.1in
Item Weight
16 Oz
Number of Pages
Xiii, 207 Pages

Über dieses Produkt

Product Information

This practice-oriented textbook shows how to utilize the huge variety of NMR experiments available today in addition to standard experiments. Intended as a practical guide for students and laboratory personnel, it treats theoretical aspects only to the extent necessary to understand the experiments and to interpret the results. The book is significantly revised and expanded for the 2nd edition, and now includes the nuclei 1H/2H, 13C, 31P, 17O, 15N, 19F, 29Si, 77Se, 113Cd, 117Sn/119Sn, 195Pt, 207Pb and a new chapter on solid state NMR. An expanded set of 50 graded problems offers invaluable help for students, practitioners and laboratory personnel alike.

Product Identifiers

Publisher
Springer Berlin / Heidelberg
ISBN-10
3540721959
ISBN-13
9783540721956
eBay Product ID (ePID)
60441655

Product Key Features

Author
Burkhard Costisella, Terence N. Mitchell
Publication Name
NMR-From Spectra to Structures : an Experimental Approach
Format
Trade Paperback
Language
English
Features
Revised
Publication Year
2007
Type
Textbook
Number of Pages
Xiii, 207 Pages

Dimensions

Item Length
9.3in
Item Height
0.2in
Item Width
6.1in
Item Weight
16 Oz

Additional Product Features

Number of Volumes
1 Vol.
Lc Classification Number
Qd71-142
Edition Description
Revised Edition
Edition Number
2
Reviews
From the reviews:"This practice-oriented textbook aims at teaching the use of NMR spectra in the elucidation of organic structures. The emphasis of the book is on practical rather than on theoritical (sic) aspects … is intended as a practical guide to today's standard NMR experiments for students and laboratory personnel. The set of 35 graded problems includes not only … for the first time in a textbook, also the most important 2D spectra (H, H and C,H correlation)." chemie Nouvelle Societe Royale de Chemie, Vol. 22(87), 2004)"The topic of this book is NMR spectroscopy on a basic level with the aim of spectral interpretation for structural elucidation. … The basic features of NMR are explained with the help of … . This book can be recommended for students … provides excellent training for the brain-based structure generator and stimulates learning of how to correlate spectral evidence with structural properties. … and offers many interesting spectral problems for self-assessment." (Stefan Berger, Anal Bioanal Chem, Vol. 381, 2005)"This book aims to teach the skill of solving the structure of organic compounds from their NMR spectra. … The description of NMR experiments is refreshingly clear, written for readers who have … . The authors also include some useful experimental tips on how to record spectra … . eminently suitable for any synthetic chemist doing a research degree. The book could also form the basis of an excellent advanced level undergraduate course … ." (Chemistry World, November, 2004)"In NMR From Spectra to Structures … have set out to provide a practical course in structure determination by NMR spectroscopy with only the essential minimum of theoretical "ballast". The first part consists of 50 pages describing methods … with brief guidance on how to assign and interpret the spectral features. The style makes for easy reading almost throughout, with carefully edited spectra and clear formulas … is very good." (Nils Schlörer, Angewandte Chemie, Vol. 43(40), 2004)"This little book is aimed at students and staff who have had little experience with NMR and need to start using it for organic structural elucidation. … In the first half, the authors … concentrate on providing a brief introduction to the different types of basic … . The second half of the book begins with a short … . I would recommend this book to students and staff who have had minimal undergraduate exposure to NMR but who need to start making … ." (Julie Niere, Chemistry in Australian Magazin of the Royal Australian Chemical Institute, July, 2004)"The book is intended to be a practical guide … . A set of thirty-five graded problems reinforces the reader's understanding of how problems of structure elucidation are solved by using NMR techniques. … This practical and comprehensed NMR handbook can be warmly recommended to graduate and undergraduate students in chemistry, biochemistry, and pharmacology, but also to experienced personnel in analytical laboratories for structure determination and elucidation." (Advances in Food Sciences, Vol. 26(2), 2004)From the reviews of the second edition:"Mitchell and Costisella … examine modern nuclear magnetic resonance (NMR) spectroscopy using purely practical aspects and applications. They look at the uses of NMR without becoming bogged down with all of the theory and mathematics behind the experiment. … both one- and two-dimensional techniques are explained. … A must read for both undergraduate and graduate students who use NMR as an analytical tool. Summing Up: Highly recommended. Lower- and upper-division undergraduates; graduate students; two-year technical program students." (S. S. Mason, CHOICE, Vol. 45 (8), 2008), From the reviews: "This practice-oriented textbook aims at teaching the use of NMR spectra in the elucidation of organic structures. The emphasis of the book is on practical rather than on theoritical (sic) aspects ... is intended as a practical guide to today's standard NMR experiments for students and laboratory personnel. The set of 35 graded problems includes not only ... for the first time in a textbook, also the most important 2D spectra (H, H and C,H correlation)." chemie Nouvelle Societe Royale de Chemie, Vol. 22(87), 2004) "The topic of this book is NMR spectroscopy on a basic level with the aim of spectral interpretation for structural elucidation. ... The basic features of NMR are explained with the help of ... . This book can be recommended for students ... provides excellent training for the brain-based structure generator and stimulates learning of how to correlate spectral evidence with structural properties. ... and offers many interesting spectral problems for self-assessment." (Stefan Berger, Anal Bioanal Chem, Vol. 381, 2005) "This book aims to teach the skill of solving the structure of organic compounds from their NMR spectra. ... The description of NMR experiments is refreshingly clear, written for readers who have ... . The authors also include some useful experimental tips on how to record spectra ... . eminently suitable for any synthetic chemist doing a research degree. The book could also form the basis of an excellent advanced level undergraduate course ... ." (Chemistry World, November, 2004) "In NMR - From Spectra to Structures ... have set out to provide a practical course in structure determination by NMR spectroscopy with only the essential minimum of theoretical "ballast". The first part consists of 50 pages describing methods ... with brief guidance on how to assign and interpret the spectral features. The style makes for easy reading almost throughout, with carefully edited spectra and clear formulas ... is very good." (Nils Schlörer, Angewandte Chemie, Vol. 43(40), 2004) "This little book is aimed at students and staff who have had little experience with NMR and need to start using it for organic structural elucidation. ... In the first half, the authors ... concentrate on providing a brief introduction to the different types of basic ... . The second half of the book begins with a short ... . I would recommend this book to students and staff who have had minimal undergraduate exposure to NMR but who need to start making ... ." (Julie Niere, Chemistry in Australian Magazin of the Royal Australian Chemical Institute, July, 2004) "The book is intended to be a practical guide ... . A set of thirty-five graded problems reinforces the reader's understanding of how problems of structure elucidation are solved by using NMR techniques. ... This practical and comprehensed NMR handbook can be warmly recommended to graduate and undergraduate students in chemistry, biochemistry, and pharmacology, but also to experienced personnel in analytical laboratories for structure determination and elucidation." (Advances in Food Sciences, Vol. 26(2), 2004) From the reviews of the second edition: "Mitchell and Costisella ... examine modern nuclear magnetic resonance (NMR) spectroscopy using purely practical aspects and applications. They look at the uses of NMR without becoming bogged down with all of the theory and mathematics behind the experiment. ... both one- and two-dimensional techniques are explained. ... A must read for both undergraduate and graduate students who use NMR as an analytical tool. Summing Up: Highly recommended. Lower- and upper-division undergraduates; graduate students; two-year technical program students." (S. S. Mason, CHOICE, Vol. 45 (8), 2008), From the reviews: "This practice-oriented textbook aims at teaching the use of NMR spectra in the elucidation of organic structures. The emphasis of the book is on practical rather than on theoritical (sic) aspects ? is intended as a practical guide to today?'s standard NMR experiments for students and laboratory personnel. The set of 35 graded problems includes not only ? for the first time in a textbook, also the most important 2D spectra (H, H and C, H correlation)." chemie Nouvelle Societe Royale de Chemie, Vol. 22(87), 2004) "The topic of this book is NMR spectroscopy on a basic level with the aim of spectral interpretation for structural elucidation. ? The basic features of NMR are explained with the help of ? . This book can be recommended for students ? provides excellent training for the brain-based structure generator and stimulates learning of how to correlate spectral evidence with structural properties. ? and offers many interesting spectral problems for self-assessment." (Stefan Berger, Anal Bioanal Chem, Vol. 381, 2005) "This book aims to teach the skill of solving the structure of organic compounds from their NMR spectra. ? The description of NMR experiments is refreshingly clear, written for readers who have ? . The authors also include some useful experimental tips on how to record spectra ? . eminently suitable for any synthetic chemist doing a research degree. The book could also form the basis of an excellent advanced level undergraduate course ? ." (Chemistry World, November, 2004) "In NMR ? From Spectra to Structures ? have set out to provide a practical course in structure determination by NMR spectroscopywith only the essential minimum of theoretical "ballast." The first part consists of 50 pages describing methods ? with brief guidance on how to assign and interpret the spectral features. The style makes for easy reading almost throughout, with carefully edited spectra and clear formulas ? is very good." (Nils Schl'rer, Angewandte Chemie, Vol. 43(40), 2004) "This little book is aimed at students and staff who have had little experience with NMR and need to start using it for organic structural elucidation. ? In the first half, the authors ? concentrate on providing a brief introduction to the different types of basic ? . The second half of the book begins with a short ? . I would recommend this book to students and staff who have had minimal undergraduate exposure to NMR but who need to start making ? ." (Julie Niere, Chemistry in Australian Magazin of the Royal Australian Chemical Institute, July, 2004) "The book is intended to be a practical guide ? . A set of thirty-five graded problems reinforces the reader?'s understanding of how problems of structure elucidation are solved by using NMR techniques. ? This practical and comprehensed NMR handbook can be warmly recommended to graduate and undergraduate students in chemistry, biochemistry, and pharmacology, but also to experienced personnel in analytical laboratories for structure determination and elucidation." (Advances in Food Sciences, Vol. 26(2), 2004), From the reviews: "This practice-oriented textbook aims at teaching the use of NMR spectra in the elucidation of organic structures. The emphasis of the book is on practical rather than on theoritical (sic) aspects ? is intended as a practical guide to today?'s standard NMR experiments for students and laboratory personnel. The set of 35 graded problems includes not only ? for the first time in a textbook, also the most important 2D spectra (H, H and C, correlation)." chemie Nouvelle Societe Royale de Chemie, Vol. 22(87), 2004) "The topic of this book is NMR spectroscopy on a basic level with the aim of spectral interpretation for structural elucidation. ? The basic features of NMR are explained with the help of ? . This book can be recommended for students ? provides excellent training for the brain-based structure generator and stimulates learning of how to correlate spectral evidence with structural properties. ? and offers many interesting spectral problems for self-assessment." (Stefan Berger, Anal Bioanal Chem, Vol. 381, 2005) "This book aims to teach the skill of solving the structure of organic compounds from their NMR spectra. ? The description of NMR experiments is refreshingly clear, written for readers who have ? . The authors also include some useful experimental tips on how to record spectra ? . eminently suitable for any synthetic chemist doing a research degree. The book could also form the basis of an excellent advanced level undergraduate course ? ." (Chemistry World, November, 2004) "In NMR ? From Spectra to Structures ? have set out to provide a practical course in structure determination by NMR spectroscopy with only the essential minimum of theoretical "ballast," The first part consists of 50 pages describing methods ? with brief guidance on how to assign and interpret the spectral features. The style makes for easy reading almost throughout, with carefully edited spectra and clear formulas ? is very good." (Nils Schl'rer, Angewandte Chemie, Vol. 43(40), 2004) "This little book is aimed at students and staff who have had little experience with NMR and need to start using it for organic structural elucidation. ? In the first half, the authors ? concentrate on providing a brief introduction to the different types of basic ? . The second half of the book begins with a short ? . I would recommend this book to students and staff who have had minimal undergraduate exposure to NMR but who need to start making ? ." (Julie Niere, Chemistry in Australian Magazin of the Royal Australian Chemical Institute, July, 2004) "The book is intended to be a practical guide ? . A set of thirty-five graded problems reinforces the reader?'s understanding of how problems of structure elucidation are solved by using NMR techniques. ? This practical and comprehensed NMR handbook can be warmly recommended to graduate and undergraduate students in chemistry, biochemistry, and pharmacology, but also to experienced personnel in analytical laboratories for structure determination and elucidation." (Advances in Food Sciences, Vol. 26(2), 2004), From the reviews: "This practice-oriented textbook aims at teaching the use of NMR spectra in the elucidation of organic structures. The emphasis of the book is on practical rather than on theoritical (sic) aspects ... is intended as a practical guide to today's standard NMR experiments for students and laboratory personnel. The set of 35 graded problems includes not only ... for the first time in a textbook, also the most important 2D spectra (H, H and C,H correlation)." chemie Nouvelle Societe Royale de Chemie, Vol. 22(87), 2004) "The topic of this book is NMR spectroscopy on a basic level with the aim of spectral interpretation for structural elucidation. ... The basic features of NMR are explained with the help of ... . This book can be recommended for students ... provides excellent training for the brain-based structure generator and stimulates learning of how to correlate spectral evidence with structural properties. ... and offers many interesting spectral problems for self-assessment." (Stefan Berger, Anal Bioanal Chem, Vol. 381, 2005) "This book aims to teach the skill of solving the structure of organic compounds from their NMR spectra. ... The description of NMR experiments is refreshingly clear, written for readers who have ... . The authors also include some useful experimental tips on how to record spectra ... . eminently suitable for any synthetic chemist doing a research degree. The book could also form the basis of an excellent advanced level undergraduate course ... ." (Chemistry World, November, 2004) "In NMR - From Spectra to Structures ... have set out to provide a practical course in structure determination by NMR spectroscopy with only the essential minimum of theoretical "ballast". The first part consists of 50 pages describing methods ... with brief guidance on how to assign and interpret the spectral features. The style makes for easy reading almost throughout, with carefully edited spectra and clear formulas ... is very good." (Nils Schlrer, Angewandte Chemie, Vol. 43(40), 2004) "This little book is aimed at students and staff who have had little experience with NMR and need to start using it for organic structural elucidation. ... In the first half, the authors ... concentrate on providing a brief introduction to the different types of basic ... . The second half of the book begins with a short ... . I would recommend this book to students and staff who have had minimal undergraduate exposure to NMR but who need to start making ... ." (Julie Niere, Chemistry in Australian Magazin of the Royal Australian Chemical Institute, July, 2004) "The book is intended to be a practical guide ... . A set of thirty-five graded problems reinforces the reader's understanding of how problems of structure elucidation are solved by using NMR techniques. ... This practical and comprehensed NMR handbook can be warmly recommended to graduate and undergraduate students in chemistry, biochemistry, and pharmacology, but also to experienced personnel in analytical laboratories for structure determination and elucidation." (Advances in Food Sciences, Vol. 26(2), 2004) From the reviews of the second edition: "Mitchell and Costisella ... examine modern nuclear magnetic resonance (NMR) spectroscopy using purely practical aspects and applications. They look at the uses of NMR without becoming bogged down with all of the theory and mathematics behind the experiment. ... both one- and two-dimensional techniques are explained. ... A must read for both undergraduate and graduate students who use NMR as an analytical tool. Summing Up: Highly recommended. Lower- and upper-division undergraduates; graduate students; two-year technical program students." (S. S. Mason, CHOICE, Vol. 45 (8), 2008)
Table of Content
Introduction.- Part I - NMR Experiments.- 1D Experiments.- 2D Experiments.- Quadrupolar Nucleus.- Experiments.- HPLC-NMR Coupling.- Appendix: Reference List.- Part II - Worked Example and Problems.- Introduction.- Worked Example.- Problems.
Copyright Date
2007
Target Audience
Scholarly & Professional
Topic
Measurement, Spectroscopy & Spectrum Analysis, Chemistry / Analytic, Chemistry / Organic
Lccn
2007-924904
Dewey Decimal
543/.66
Dewey Edition
22
Illustrated
Yes
Genre
Technology & Engineering, Science

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